1994
DOI: 10.1016/0167-2738(94)90138-4
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Polymer electrolytes based on crosslinked silylated poly-vinyl-ether and lithium perchlorate

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Cited by 11 publications
(44 citation statements)
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“…Each polymer host was studied with varying amounts of LiTFSI, over the temperature range from room temperature to 70 • C. Equipment 1 H, 13 C NMR were obtained on a Bruker AC300 and 29 Si NMR spectra were recorded on a Varian Unity 500 spectrometer. CDCl 3 was used as the solvent and TMS was the internal reference for 1 H, 13 C NMR. 29 Si chemical shifts are reported relative to an external TMS standard.…”
Section: Polymer/litfsi Complex Preparationmentioning
confidence: 99%
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“…Each polymer host was studied with varying amounts of LiTFSI, over the temperature range from room temperature to 70 • C. Equipment 1 H, 13 C NMR were obtained on a Bruker AC300 and 29 Si NMR spectra were recorded on a Varian Unity 500 spectrometer. CDCl 3 was used as the solvent and TMS was the internal reference for 1 H, 13 C NMR. 29 Si chemical shifts are reported relative to an external TMS standard.…”
Section: Polymer/litfsi Complex Preparationmentioning
confidence: 99%
“…29 Si chemical shifts are reported relative to an external TMS standard. 13 C NMR was recorded as proton decoupled spectra, and 29 Si NMR was recorded using an inverse gate pulse sequence with a relaxation delay of 30 s. Impedance measurements were performed under computer control using a Princeton Applied Research model 273A potentiostat/galvanostat, Princeton Applied Research model 1025 frequency response analyzer for frequency control (75 Hz to 100 kHz), and Princeton Applied Research PowerSine impedance software for data acquisition. Subsequently, the data obtained was analyzed on a PC with Microsoft Excel.…”
Section: Polymer/litfsi Complex Preparationmentioning
confidence: 99%
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“…7 Recognizing that the ionic conductivity of PEObased electrolyte is facilitated in the amorphous phase, significant research efforts have been devoted in obtaining a polymer structure having a highly flexible backbone and a larger proportion of the amorphous phase. For instance, several comb-like polymers, 10 copolymers 11 and crosslinked polymers, 12 have been prepared, and their charge transport properties have been investigated. However, most of these polymers require a nontrivial synthetic process, and this is a serious drawback for practical applications.…”
Section: Introductionmentioning
confidence: 99%