Photocatalytic evaluation of CuO and ZnO crystallites synthesized hydrothermally using binary eugenol/iso-eugenol mixtures: isomer effects on the capping propensity of biogenic agents

Jan, Tabee; Raheem, Shabnam; Sawant, S. V.; Manolikar, T. V.; Sakate, S. S.; Pardeshi, S. K.; Jagtap, R. M.; Rizvi, Masood Ahmad

doi:10.1039/d3nj05237k

New J. Chem.

2024

DOI: 10.1039/d3nj05237k

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Photocatalytic evaluation of CuO and ZnO crystallites synthesized hydrothermally using binary eugenol/iso-eugenol mixtures: isomer effects on the capping propensity of biogenic agents

Tabee Jan,

Shabnam Raheem,

S. V. Sawant

et al.

Abstract: Isomer effects on the capping propensity of biogenic agents used in nanomaterial synthesis.

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2024

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Cited by 3 publications

References 80 publications

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Oxalate and adipate mediated fabrication of CuO nanocrystallites for their electrochemical and supercapacitance studies

Sawant,

Manolikar,

Babar

et al. 2024

Discov. Chem.

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Cupric oxide (CuO) has been comprehensively studied in the field of electrochemistry due to its high Tc-Superconducting property. The present work focus on two different CuO materials i.e. CuO-1 and CuO-2 nanocrystallites which are successfully synthesized from their oxalate and adipate precursors respectively. The calcination temperature for the synthesis of CuO from their precursors is ascertained by TGA analysis of the dicarboxylates. Both the CuO materials are thoroughly characterized by SEM–EDS, XRD, IR and XPS spectroscopic techniques. As a candidate for supercapacitor electrode material, CuO-1/C and CuO-2/C showed a specific capacitance of 4.15 F/g and 22.24 F/g using cyclic voltammetry, 10.4 F/g and 46.6 F/g using GCD curves respectively at a current density of 1 A/g. Also, the CuO-1/C and CuO-2/C showed a specific energy density (Es) 1.59 Wh kg−1 and 0.36 Wh kg−1 at a specific power density (Ps) of 0.02 kW kg−1 and 0.025 kW kg−1 respectively. Moreover, the CuO-2/C exhibits ≈ 96.1% coulombic efficiency following 1000 cycles, whereas, CuO-1/C lags in coulombic efficiency with only 51.8%. As a better candidate, CuO-2/C exhibited excellent rate capability with an outstanding cycling stability of 93.7% retention after 1,000 cycles. The factors contributing to the significant specific capacitance of CuO-2/C along with better stability and reproducibility are its low electrolyte resistance Rs (2.47Ω) and charge transfer resistance Rct (1.01 Ω).

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Oxalate and adipate mediated fabrication of CuO nanocrystallites for their electrochemical and supercapacitance studies

Sawant,

Manolikar,

Babar

et al. 2024

Discov. Chem.

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Precursor effect on the hydrothermal synthesis of pure ZnO nanostructures and enhanced photocatalytic performance for norfloxacin degradation

Resende Leite,

Colombo,

Eduardo Bimbi Júnior

et al. 2024

Chemical Engineering Journal

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Design and development of symmetric aromatic bischalcogenide-based photocatalysts for water treatment application: a concise study of diphenyl diselenide polypyrrole nanocatalysis

Jan,

Raheem,

Rizvi

2024

Nanoscale Adv.

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Photocatalytic evaluation of CuO and ZnO crystallites synthesized hydrothermally using binary eugenol/iso-eugenol mixtures: isomer effects on the capping propensity of biogenic agents

Abstract: Isomer effects on the capping propensity of biogenic agents used in nanomaterial synthesis.

Cited by 3 publications

References 80 publications

Oxalate and adipate mediated fabrication of CuO nanocrystallites for their electrochemical and supercapacitance studies

Oxalate and adipate mediated fabrication of CuO nanocrystallites for their electrochemical and supercapacitance studies

Precursor effect on the hydrothermal synthesis of pure ZnO nanostructures and enhanced photocatalytic performance for norfloxacin degradation

Design and development of symmetric aromatic bischalcogenide-based photocatalysts for water treatment application: a concise study of diphenyl diselenide polypyrrole nanocatalysis

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