“…(2) A, V¼3349.4(5) A 3 , Z¼4, r(calcd)¼1.179 Mg m À3 , F(000)¼1264, m¼0.077 mm À1 , 7656 reflections (2q max ¼55 ), 7656 unique [R int ¼0.000], 383 parameters, 1 restraints, R1 (for 6137 I>2s(I))¼ 0.049, wR2 (all data)¼0.105, S¼1.04, largest diff. peak and hole 0.208 and À0.148 e A À3 , x¼À0.0(10), y¼0.3 (5).…”