Abstract:The synthesis of isopelletierine from A'-piperideine and acetoacetic acid was investigated in the p H region 1 to 12. Paper chromatography was used t o analyze the reaction mixtures. Depending on reaction time fair to good yields were obtained over the p H range 2 to 12. The experimental data are discussed in the light of two mechanisms proposed by Schiipf et a12. Several methods have been described for the synthesis of isopelletierine. Except for the synthesis from A'-piperideine, originated by Schiipfl* 2 , … Show more
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