Ionization sampling resolution and relativistic rise at 15 GeV/c were compared at different pressures in neon, argon, krypton, xenon and pure hydrocarbons, using a detector consisting of 64 samples of 4 cm and a drift space of up to 50 cm. Best results were obtained for Ir/p separation in neon (> 6.70) and for e/It separation in xenon (> 4.8o). Pure ethylene and propane were comparable to argon mixtures for ~r/p separation, but the corresponding e/~r separation suffered from a lower relativistic rise. The signal attenuation by electron attachment was more pronounced in heavier hydrocarbons. Drift velocity measurements are presented and E/p limits imposed by requirements of dE/dx resolution are discussed.