Performance and calibration of the Flash DSC 1, a new, MEMS-based fast scanning calorimeter

Poel, Geert Vanden; Istrate, Daniel; Magoń, A.; Mathot, Vincent

doi:10.1007/s10973-012-2722-7

Cited by 104 publications

(57 citation statements)

References 21 publications

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“…But for the small sample shown in Fig. 1 the thermal lag should be a concern when rates above 10,000 K s À1 are used [26,33], which is not the case of experiment described in this work. The reason for the dramatic broadening of the relaxation peak is not known yet.…”

Section: Discussionmentioning

confidence: 87%

Enthalpy relaxation of selenium observed by fast scanning calorimetry

et al. 2015

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Section: Discussionmentioning

confidence: 87%

Enthalpy relaxation of selenium observed by fast scanning calorimetry

et al. 2015

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“…The enthalpy of fusion (DH m ) measured by conventional DSC was used as a reference value according to Eq. (1) [20]: Note that more than one crystallization peak is visible for all BMGs investigated in Fig. 1.…”

Section: Thermo-analytical Measurementsmentioning

confidence: 86%

Characterization of bulk metallic glasses via fast differential scanning calorimetry

et al. 2014

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“…A flow A. Dhotel et al rate of 20 mL min -1 was selected for optimal performances [31]. Thin films of PS and PETg were prepared by pressing pellets between two aluminum sheets.…”

Section: Flash Differential Scanning Calorimetry (F-dsc)mentioning

confidence: 99%

Combining Flash DSC, DSC and broadband dielectric spectroscopy to determine fragility

Dhôtel

Rijal

Delbreilh

et al. 2015

J Therm Anal Calorim

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New experimental results focused on Flash DSC, DSC and broadband dielectric spectroscopy investigations are reported in this work. The fictive temperatures and fragility indexes are estimated from Flash DSC experiments and compared to values obtained from classical DSC. The consistency of the Tool-NarayanaswamyMoynihan model and fragility concept is then investigated over a large range of cooling rates. Indeed, the Flash DSC allows exploring thermal properties of materials over a continuous and broad range of heating and cooling rates, complementary to rates usually available with DSC. The reliability of investigations is also demonstrated by comparing results obtained from two model amorphous polymeric systems: polystyrene and poly(ethylene terephthalate)-glycol. The temperature dependence of the cooling rate obtained by Flash DSC and DSC is also compared to the temperature dependence of the relaxation times obtained from broadband dielectric spectroscopy, experiment considered as the reference concerning the fragility measurements. The comparison of these two dependencies implies a better understanding about the origin of the temperature dependence of the cooling rate.

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Performance and calibration of the Flash DSC 1, a new, MEMS-based fast scanning calorimeter

Cited by 104 publications

References 21 publications

Enthalpy relaxation of selenium observed by fast scanning calorimetry

Enthalpy relaxation of selenium observed by fast scanning calorimetry

Characterization of bulk metallic glasses via fast differential scanning calorimetry

Combining Flash DSC, DSC and broadband dielectric spectroscopy to determine fragility

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