Pentaerythritol Derivatives. II. 3-Halomethyl-3-hydroxymethyl Oxetanes<sup>1</sup>

Issidorides, Costas H.; Gulen, Riza C.; Aprahamian, Nazar S.

doi:10.1021/jo01115a018

Cited by 10 publications

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“…Owing to the limitation of the raw material source, the chlorinated alcohol method is not used widely, but the process can reduce the production cost and environmental pollution. Some researchers have conducted research on the use of LBC 8–13. Zheng et al.…”

Section: Introductionmentioning

confidence: 99%

Facile and Rapid Synthesis of Neopentyl Glycol in a Continuous‐Flow Microreactor

Yang

Yue

et al. 2021

Chem Eng & Technol

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Neopentyl glycol (NPG) synthesis by condensation disproportionation of formaldehyde and isobutyraldehyde (IBD) with sodium hydroxide as catalyst was studied in a continuous‐flow microreactor under various experimental conditions, such as reaction temperature, residence time, and the molar ratio of reactants. All the conditions were determined by Box‐Behnken experimental design and the response surface method based on the preferred range selected by single‐factor experiments. For comparison, NPG was synthesized by condensation disproportionation of the same reactants in a batch reactor. The results showed that higher NPG yield and shorter residence time were achieved in a continuous‐flow microreactor than in a batch reactor when the other experimental conditions were similar.

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Section: Introductionmentioning

confidence: 99%

Facile and Rapid Synthesis of Neopentyl Glycol in a Continuous‐Flow Microreactor

Yang

Yue

et al. 2021

Chem Eng & Technol

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“…Tribromide 1 was prepared in 68% yield from the reaction of pentaerythritol with 40% aqueous HBr solution in acetic acid [10]. Using a modified literature procedure, the ring closure reaction to form dibromide 2 successfully proceeded in the presence of sodium ethoxide, affording 2 in 62% yield [11]. Treatment of 2 with >2.0 equiv.…”

Section: Introductionmentioning

confidence: 99%

Synthesis and structural characterization of ruthenium(II) complexes bearing phosphine-pyrazolyl based tripod ligands

Tan

Zhao

2007

Journal of Organometallic Chemistry

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“…D. R. LeveringReceived July9, 1959 The synthesis of esters from olefins, carbon monoxide, and alcohols using metal carbonyls,…”

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confidence: 99%

Notes: 7-Phenyl-2:6:8-trioxaspiro(3,5)-nonane: A High Yield Reduction with Lithium Aluminum Hydride

Nassar¹,

Issidorides²

1959

J. Org. Chem.

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Pentaerythritol Derivatives. II. 3-Halomethyl-3-hydroxymethyl Oxetanes¹

Cited by 10 publications

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Facile and Rapid Synthesis of Neopentyl Glycol in a Continuous‐Flow Microreactor

Facile and Rapid Synthesis of Neopentyl Glycol in a Continuous‐Flow Microreactor

Synthesis and structural characterization of ruthenium(II) complexes bearing phosphine-pyrazolyl based tripod ligands

Notes: 7-Phenyl-2:6:8-trioxaspiro(3,5)-nonane: A High Yield Reduction with Lithium Aluminum Hydride

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Pentaerythritol Derivatives. II. 3-Halomethyl-3-hydroxymethyl Oxetanes1

Cited by 10 publications

References 0 publications

Facile and Rapid Synthesis of Neopentyl Glycol in a Continuous‐Flow Microreactor

Facile and Rapid Synthesis of Neopentyl Glycol in a Continuous‐Flow Microreactor

Synthesis and structural characterization of ruthenium(II) complexes bearing phosphine-pyrazolyl based tripod ligands

Notes: 7-Phenyl-2:6:8-trioxaspiro(3,5)-nonane: A High Yield Reduction with Lithium Aluminum Hydride

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Pentaerythritol Derivatives. II. 3-Halomethyl-3-hydroxymethyl Oxetanes¹