Peer Review #1 of "X-ray diffraction and theoretical study of the transition 2H-3R polytypes in Nb1+xSe2 (0 < x < 0.1) (v0.1)"
Abstract:Single crystals of 2H and 3R niobium diselenide were grown by a chemical transport reaction. The current determinations by single crystals X-ray diffraction reveal a nonstoichiometric composition. The structures are built from Se-Nb-Se slabs with Nb in trigonal prismatic coordination whereas the extra or additional Nb atoms are located in the octahedral holes between the slabs giving rise to the formula 2H and 3R-Nb 1+x Se 2 with 0.07< x <0.118. In particular, vacancy and Nb-Nb interactions may play an importa… Show more
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