Abstract:Palladium supported MCM-41 molecular sieves with Si/Pd (molar) ratios of 400, 200, 100 and 50 were synthesized by hydrothermal method. All catalysts characterized by various analytical and spectroscopic techniques, viz, XRD, N 2 sorption, TEM, DRUV-VIS, Raman. XRD at low angle and high angle studies suggest that the substitution of palladium and presence of palladium oxide phase in the silicate tetrahedral framework structure of MCM-41. TEM investigations con¯rm the highly ordered cubic structure with irregula… Show more
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