“…Then, it decreases. Its magnitude and behavior are similar to that of Ni 0.5 Zn 0.5 Cr 0.5 Fe 1.5 O 4 nanoparticles dielectrically studied by Tan et al 69 This evolution was due to the decrease in polarization with frequency. 70 Four kinds of polarizations, namely, interfacial, dipolar, electronic, and ionic polarization have an obvious effect on the dielectric constant.…”
Section: Impedance Measurementsupporting
confidence: 84%
“…16(a)). A similar anomaly was found by Mohamed et al 73 for a nanocomposite PANI-Ni 0.5 Zn 0.5 Fe 1.5 Cr 0.5 O 4 around 333 K and by Tan et al 74 at 305 K. This peak may be attributed to local polarization 75 and its wide dispersion indicates the diffuse character of phase transition that the material undergoes. 76 With increasing frequency, the dielectric maxima shi to higher temperatures.…”
In the present study, the structural, morphological, electrical, and dielectric properties of Ni0.6Zn0.4Fe1.5Al0.5O4 annealed at 600 °C, 900 °C, and 1200 °C were investigated.
“…Then, it decreases. Its magnitude and behavior are similar to that of Ni 0.5 Zn 0.5 Cr 0.5 Fe 1.5 O 4 nanoparticles dielectrically studied by Tan et al 69 This evolution was due to the decrease in polarization with frequency. 70 Four kinds of polarizations, namely, interfacial, dipolar, electronic, and ionic polarization have an obvious effect on the dielectric constant.…”
Section: Impedance Measurementsupporting
confidence: 84%
“…16(a)). A similar anomaly was found by Mohamed et al 73 for a nanocomposite PANI-Ni 0.5 Zn 0.5 Fe 1.5 Cr 0.5 O 4 around 333 K and by Tan et al 74 at 305 K. This peak may be attributed to local polarization 75 and its wide dispersion indicates the diffuse character of phase transition that the material undergoes. 76 With increasing frequency, the dielectric maxima shi to higher temperatures.…”
In the present study, the structural, morphological, electrical, and dielectric properties of Ni0.6Zn0.4Fe1.5Al0.5O4 annealed at 600 °C, 900 °C, and 1200 °C were investigated.
“…1 In the last few years there has been increasing interest in mixed ferrites, because of their interesting physical, chemical, and structural properties, and remarkably promising applications. 2 The spinel ferrites are an important group of magnetic materials, because of their useful magnetic properties, especially in the radiofrequency region, physical flexibility, high electrical resistivity, mechanical hardness, and chemical stability. Because of their excellent properties, much attention has also been devoted to mixed spinel ferrites, which are mainly used in electrical devices and as catalysts.…”
Titanium-Catalyzed Intermolecular Hydroaminoalkylation of ConjugatedDienes. -For the first time the new and highly atom-efficient reaction for the synthesis of homoallylic amines from readily available 1,3-butadienes is presented. The scope of the reaction is still limited [e.g. reaction of (If), (Vb), and (VIIIb)]. Aliphatic dienes (XI) react much more regioselectively than the aromatic ones. -(PREUSS, T.; SAAK, W.; DOYE*, S.; Chem. -Eur.
In the present study, Al-Cd ferrites of nominal composition AlxCd1−xFe2O4 (x = 0-0.5) were prepared by coprecipitation method. The effect of Al +3 additive on the structural, optical, and magnetic properties of the as-prepared Al-Cd ferrites was investigated. Samples were characterized by X-ray diffraction, scanning electron microscopy, the Fourier transform infrared spectroscopy, UV spectroscopy and vibrating sample magnetometer techniques. The magnetic analysis indicated that all of the samples in different compositions showed ferromagnetic behavior. Along with the X-ray diffraction patterns, the formation of single-phase cubic spinel structure and the lattice parameter were identified in the range of 8.6492-8.6984 Å. Scanning electron microscopy measurements showed that the smallest ferrite nanoparticles were obtained when the stoichiometric composition factor (x) value was 0.4. As an additional characterization, the Fourier transform infrared spectra was investigated, and the characteristic absorption, bands belonging to ferrite nanoparticles were identical around 530 cm −1 and 430 cm −1. The tetrahedral and the octahedral complex formation was proved by the observation of higher frequency (ν1), and lower frequency (ν2) bands by Fourier transform infrared method, respectively. UV-Vis characterization performed for the determination of Eg values depending on changing Al concentration and found as 2.07-2.24 eV. From the magnetic measurements, all the Al-doped Cd ferrites exhibit S-shaped narrow hysteresis loops revealing soft ferromagnetic nature of the formed ferrites.
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