We report on the magnetic anisotropy (MA) and magnetoresistance (MR) properties of [Co (t Co )/Au (t Au )] θ N multilayers prepared by changing the incident angle of deposition, θ , thicknesses t Co and t Au of Co and Au layers, respectively, and number of bilayers, N, while keeping N × t Co fixed at 20 nm. Although all of the multilayers showed MAs at low applied magnetic fields, H, and room temperature, the ones deposited at θ = 45°showed remarkable mgnetic anisotropies, which is further enhanced upon magnetic annealing. The [Co (1 nm)/Au (2 nm)] 45 20 multilayer showed a maximum MR of 2.1% at room temperature and H = 1 kOe. Moreover, for the same field H and current I, the transverse (H ⊥ I) MR is always larger than the longitudinal (H I ) MR. Index Terms-Co/Au multilayer, magnetic anisotropy (MA), magnetoresistance (MR), oblique angle deposition. Belaid Moa received the Ph.D. degree in computer science from the University of Victoria, Victoria, BC, Canada, the M.Eng. degree in electronics and signal processing from École Nationale Supérieure d'électronique, d'électrotechnique, d'informatique, d'hydraulique et des Télécommunications, Toulouse, France, and the B.Sc. degree in electrical engineering from École Hassania des Travaux Publics, Casablanca, Morocco.He is currently a Research Computing Staff with Compute , as an Assistant Professor, in 2007, where he became an Associate Professor in 2013. His current research interests include use of synchrotron X-ray sources to study nanoscale structure and dynamics in a wide range of materials systems and devices, from liquids and polymers to magnetic materials, charge density wave systems and battery materials.