2022
DOI: 10.26434/chemrxiv-2022-5lcrq
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Order beyond a monolayer: the story of two 4,4’-bipyridine layers on the Sb(111) | ionic liquid interface

Abstract: The interface between semi-metallic Sb(111) electrode and ionic liquid with 4,4’-bipyridine addition has been studied. Using in situ scanning tunnelling microscopy and electrochemical impedance spectroscopy, the desorption of 4,4’-bipyridine was demonstrated and a dense underlying structure, formed below a sparse self-assembled monolayer, was visualized. The first SAM layer in contact with the electrode consisted of tightly packed ordered rows, which fine structure has been identified with density functional t… Show more

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