Optimization of the macroporous resin-based adsorption of apple polyphenol through response surface methodology

Fu, Ruimin; Wang, Yaya; Yu, Feng; Wu, Xiaowei; Gu, Yu; Wu-ling, Chen

doi:10.1080/02772248.2015.1123490

Cited by 9 publications

(4 citation statements)

References 27 publications

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“…As shown in the picture, at the small elution volume, the slower the flow velocity, the poorer the desorption efficiency. The reason for this phenomena was that the low flow rate might extend the operation cycle and had adverse effects on production (Fu et al., 2016). The efficiency declined when the flow rate was more than 1.6 mL/min, which due to the short contact time.…”

Section: Resultsmentioning

confidence: 99%

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Response surface optimization of the water immersion extraction and macroporous resin purification processes of anhydrosafflor yellow B from Carthamus tinctorius L.

Zhou

Fangma

Jin

et al. 2020

Journal of Food Science

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In this study,based on a developed high performance liquid chromatographic quantitative method, the suitable extraction and purification conditions of anhydrosafflor yellow B (AHSYB) from safflower were determined by response surface methodology. The optimal water immersion extraction parameters were as follows: liquid to solid ratio of 22:1; extraction temperature of 75°C; extraction time of 35 min. Under these conditions, the maximum extraction yield of AHSYB reached 0.465%. The aqueous extract was further purified by HPD-300 macroporous resin. The optimum adsorption conditions were: pH 2.8; adsorption flow rate of 1.9 mL/min; solution concentration of 0.06 g/mL. The optimum desorption conditions were: ethanol concentrations of 74%; desorption flow rate of 1.6 mL/min; elution volume of 4.4 BV. Under these conditions, the maximum adsorption ratio and desorption ratio reached 1.095 and 0.906 mg/g, respectively. The content of AHSYB reached 6.83%, which was 2.91 times higher than that before purification.

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Section: Resultsmentioning

confidence: 99%

“…It had been reported in the literature, pH, flow rate, and concentration of loading solution are the main influential factors of dynamic adsorption (Fu et al., 2016). And the ethanol concentration, desorption flow rate, elution volume may affect dynamic desorption (Wu, Wang, He, Li, & Wang, 2018).…”

Section: Methodsmentioning

confidence: 99%

Response surface optimization of the water immersion extraction and macroporous resin purification processes of anhydrosafflor yellow B from Carthamus tinctorius L.

Zhou

Fangma

Jin

et al. 2020

Journal of Food Science

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“…After selecting the most suitable macroporous resin for the purification of naringin, the effects of loading concentration, loading flow rate, and sample PH on the adsorption rate of naringin and the effect of ethanol concentration on the desorption rate of naringin were investigated. The optimum conditions for the purification of naringin with macroporous resins have been previously determined [ 20 , 21 ].…”

Section: Methodsmentioning

confidence: 99%

Optimisation of the Extraction Process of Naringin and Its Effect on Reducing Blood Lipid Levels In Vitro

Meng²,

Yan³

et al. 2023

Molecules

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The naringin extraction process was optimised using response surface methodology (RSM). A central component design was adopted, which included four parameters: extraction temperature (X1), material–liquid ratio (X2), extraction time (X3), and ultrasonic frequency (X4) of 74.79 °C, 1.58 h, 1:56.51 g/mL, and 28.05 KHz, respectively. Based on these optimal extraction conditions, naringin was tested to verify the model’s accuracy. Naringin yield was 36.2502 mg/g, which was equivalent to the predicted yield of 36.0124 mg/g. DM101 macroporous adsorption resin was used to purify naringin. The effects of loading concentration, loading flow rate, and sample pH on the adsorption rate of naringin and the effect of ethanol concentration on the desorption rate of naringin were investigated. The optimum conditions for naringin purification using macroporous resins were determined. The optimal loading concentration, sample solution pH, and loading flow rate were 0.075 mg/mL, 3.5, and 1.5 mL/min, respectively. Three parallel tests were conducted under these conditions, and the average naringin yield was 77.5643%. Naringin’s structure was identified using infrared spectroscopy and nuclear magnetic resonance. In vitro determination of the lipid-lowering activity of naringin was also conducted. These results showed that naringin has potential applications as a functional food for lowering blood lipid levels.

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“…This method allows for the isolation or separation of individual polyphenols or the enrichment of specific polyphenol subclasses from crude phenolic extracts via adjusting the optimal adsorption conditions for individual compounds. Kammerer et al [74] used food-grade acrylic adsorbents for the separation and purification of phenolic compounds from crude plant extracts and found that grading of the extracts based on the hydrophilicity of the phenolics was possible and resin adsorption properties were required to improve the recovery and fractionation potential of the phenolic compounds isolated from plant material., Fu et al [75] used a macroporous adsorption resin to adsorb and purify apple polyphenols under the following optimal adsorption conditions: HPD-100 MR, 2.5 BV/hr flow rate, 0.44 Abs adsorption concentration, and pH 2.13. Under these conditions, the polyphenol adsorption rate reached 95.27%.…”

Section: Resin Adsorption Extraction Methodsmentioning

confidence: 99%

Recent Technologies for the Extraction and Separation of Polyphenols in Different Plants: A Review

Hu¹,

Yan²,

Chen³

et al. 2022

Journal of Renewable Materials

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Optimization of the macroporous resin-based adsorption of apple polyphenol through response surface methodology

Cited by 9 publications

References 27 publications

Response surface optimization of the water immersion extraction and macroporous resin purification processes of anhydrosafflor yellow B from Carthamus tinctorius L.

Response surface optimization of the water immersion extraction and macroporous resin purification processes of anhydrosafflor yellow B from Carthamus tinctorius L.

Optimisation of the Extraction Process of Naringin and Its Effect on Reducing Blood Lipid Levels In Vitro

Recent Technologies for the Extraction and Separation of Polyphenols in Different Plants: A Review

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