Optimization of the Extraction Technology of Chlorogenic Acid in Honeysuckle Response Surface Method

Cui, Tingting; Wang, Chao; Shan, Chang-Song; Wu, Peng

doi:10.4236/oalib.1100941

Cited by 4 publications

(4 citation statements)

References 17 publications

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“…Graphical representations of the regression equation (3‐D RS and 2‐D C plots) are very useful for evaluating independent–dependent (factor–response) variable relationships. A circular 2‐D C plot indicates insignificant interactions of parameters, whereas an elliptical 2‐D C plot depicts significant interactions of variables (Cui et al., 2014). The CA yield slightly decreased at first and then increased steadily as A increased and B decreased.…”

Section: Resultsmentioning

confidence: 99%

Ultrasonic‐assisted extraction of bioactive chlorogenic acid from heilong48 soybean variety: Parametric optimization and evaluation of physicochemical and bioactive properties

Akpabli‐Tsigbe

Ekumah

et al. 2022

Food Science & Nutrition

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Chlorogenic acid (CA), especially that found in soybeans, is a rich bioactive compound but has received very little attention in research settings in past decades. Ultrasonic‐assisted extraction (UAE) could be an efficient method to increase CA release from soybeans. Hence, this study aimed to optimize UAE parameters for CA extraction from heilong48 soybean (HS) variety and evaluate the physicochemical and bioactive properties of the soybean. Optimization of ultrasound parameters with a Box–Behnken design found a frequency of 20.0 kHz, a power density of 30.0 W/L), a temperature of 37.9°C, and a time of 28.0 min to be the best conditions, which gave a CA yield of 5.007 ± 0.033 mg/g and 2,2‐diphenyl‐1‐picrylhydrazyl (DPPH) radical scavenging activity of 93.197 ± 0.213 μmol of AA eq/g dry sample; these were higher than those of a non–ultrasound‐treated (raw) HS sample (CA yield of 1.627 ± 0.528 mg/g and DPPH radical scavenging activity of 10.760 ± 0.207 μmol of AA eq/g dry sample). A satisfactory model was obtained. Scanning electron microscopy results confirmed the structural changes of the HS variety caused by the optimized UAE parameters. High total polyphenol contents (TPCs; 4.726 ± 0.002 mg GAE/g) and total phenolic acids (1.883 ± 0.005 mg GAE/g) and low total flavonoid contents (0.040 ± 0.008 mg RE/g) were obtained. A positive linear correlation between antioxidant activity and TPC was established. A protein–phenolic interaction in the HS variety was observed. The results established that polyphenols should be considered a significant component of the HS variety. Likewise, the HS variety could be used for CA extraction.

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Section: Resultsmentioning

confidence: 99%

Ultrasonic‐assisted extraction of bioactive chlorogenic acid from heilong48 soybean variety: Parametric optimization and evaluation of physicochemical and bioactive properties

Akpabli‐Tsigbe

Ekumah

et al. 2022

Food Science & Nutrition

View full text Add to dashboard Cite

show abstract

“…Representations of regression equation graphically (3‐D RS and 2‐D C plots) are very useful to evaluate independent‐dependent (factor‐response) variables relationship. Circular 2‐D C plot indicates insignificant interactions of parameters, while elliptical 2‐D C plot depicts significant interactions of variables (Cui et al., 2014). CA yield slightly decreased at first and then increased steadily as A increased and B decreased.…”

Section: Resultsmentioning

confidence: 99%

Single‐frequency ultrasonic extraction of bioactive chlorogenic acid from heilong48 soybean variety: Parametric optimization and comprehensive evaluation of physicochemical and bioactive properties

Akpabli‐Tsigbe

Ekumah

et al. 2021

Food Science & Nutrition

View full text Add to dashboard Cite

Chlorogenic acid (CA), especially that found in soybean, is a rich bioactive compound but has received very little attention in research settings in past decades. Ultrasonic‐assisted extraction (UAE) could be an efficient method to increase CA release from soybean. Hence, this study aimed to optimize UAE parameters for CA extraction from heilong48 soybean (HS) variety with comprehensive physicochemical and bioactive properties evaluation. Optimization of ultrasound parameters with Box‐Behnken design (BBD) found frequency (20.0 kHz), power density (30.0 W/L), temperature (37.9℃), and time (28.0 min) as the significant optimized parameters, which gave CA yield of 5.007 ± 0.033 mg/g and DPPH of 93.197 ± 0.213 μmol AA eq/g dry sample and were higher than that of nonultrasound‐treated (raw) HS sample (CA yield, 1.627 ± 0.528 mg/g, and DPPH, 10.760 ± 0.207 μmol AA eq/g dry sample). A satisfactory model was obtained. SEM results confirmed the structural alterations of HS variety caused by the optimized UAE parameters. High TPC (4.726 ± 0.002 mg GAE/g), TPA (1.883 ± 0.005 mg GAE/g), and low TFC (0.040 ± 0.008 mg RE/g) were obtained. A positive linear correlation between antioxidant activity and TPC was established. Protein–phenolic interaction in HS variety was observed. The results proposed that polyphenols should be considered as a significant component of HS variety. Likewise, HS variety could be utilized for CA extraction.

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“…Asam parahidroksibenzoat stabil hingga suhu 90 o C (Castada et al, 2020). Asam klorogenat stabil hingga suhu 70 o C (Cui et al, 2014). Kulit buah naga merah yang juga diketahui mengandung asam galat, asam ferulat, asam parahidroksibenzoat yang tahan terhadap suhu tinggi (Suleria et al, 2020).…”

Section: Aktivitas Antioksidanunclassified

Kualitas Es Puter dengan Penambahan Bubur Kulit Buah Naga Merah Bagian Dalam (Hylocereus polyrhizus) dan Ekstrak Pektinnya sebagai Agen Penstabil

Kho,

Swasti,

Pranata

2022

J. Apl. Teknol. Pang.

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Es puter adalah salah satu jenis frozen dessert yang mirip dengan es krim, namun menggunakan santan kelapa sebagai sumber lemaknya. Es puter umumnya memiliki kristal es yang kasar, sehingga diperlukan agen penstabil untuk mencegah pembentukan kristal es yang kasar dan agar tidak mudah meleleh. Kulit buah naga merah diketahui mengandung pektin sebanyak 10,79%, sehingga berpotensi digunakan sebagai agen penstabil. Penelitian ini menggunakan bubur kulit buah naga merah bagian dalam dengan konsentrasi 5, 10, dan 15% dan ekstrak pektinnya ke dalam produk es puter. Es puter dengan penstabil CMC juga dibuat sebagai pembanding. Karakteristik berupa kadar lemak, kadar protein, total padatan, kadar serat tak larut, kadar serat larut, total fenolik, aktivitas antioksidan, waktu leleh, overrun, angka lempeng total, dan keberadaan Salmonella es puter dianalisis dengan menggunakan rancangan acak lengkap dan diuji lanjut dengan Duncan Multiple Range Test. Kesimpulannya, penambahan 10% bubur kulit buah naga merah bagian dalam dan ekstrak pektinnya mampu menghasilkan es puter yang terbaik. Produk perlakuan terbaik memiliki kadar lemak sebesar 10,61%, kadar protein 1,95%, total padatan 30,99%, kadar serat tak larut 0,90%, kadar serat larut 1,12%, total fenolik 28,55 mg GAE/100 g, aktivitas antioksidan 80,42%, waktu leleh 1039 detik/30 gram es puter, overrun 40,86%, angka lempeng total 5,3 x 102 CFU/g, dan negatif untuk keberadaan Salmonella.

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Optimization of the Extraction Technology of Chlorogenic Acid in Honeysuckle Response Surface Method

Cited by 4 publications

References 17 publications

Ultrasonic‐assisted extraction of bioactive chlorogenic acid from heilong48 soybean variety: Parametric optimization and evaluation of physicochemical and bioactive properties

Ultrasonic‐assisted extraction of bioactive chlorogenic acid from heilong48 soybean variety: Parametric optimization and evaluation of physicochemical and bioactive properties

Single‐frequency ultrasonic extraction of bioactive chlorogenic acid from heilong48 soybean variety: Parametric optimization and comprehensive evaluation of physicochemical and bioactive properties

Kualitas Es Puter dengan Penambahan Bubur Kulit Buah Naga Merah Bagian Dalam (Hylocereus polyrhizus) dan Ekstrak Pektinnya sebagai Agen Penstabil

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