Optical and Electrical Properties of A3[VS4] (A = Na, K) Synthesized via a Straightforward and Scalable Solid-State Method
Mohammad R. Ghazanfari,
Laura Vittadello,
Stephanie Bachmann
et al.
Abstract:Two literature-known sulfido vanadates, Na3[VS4] and K3[VS4], were obtained
through a straightforward
and scalable synthetic method. Highly crystalline powders of both
compounds were obtained from the homogeneous molten phases of starting
materials via acomparably rapidsolid-state technique.
Low-temperature structure determination, ambient temperature powder
diffraction, and solid-state NMR spectroscopy verify previous structural
reports and indicate purity of the obtained samples. Both compounds
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