Opportunities to explore large OSDA in zeolite synthesis: New routes created from the ITQ lab

Studies on the Conversion of FAU Zeolites to SSZ-13: The Rate Advantage of Having Both Si and Al in the FAU Reagent

“…Radio-frequency (RF) pulse powers of 62.5 kHz were used for 1 H and 13 C channels for MAS or CPMAS NMR data acquisition. Chemical shifts were externally calibrated with respect to TMS (tetramethysilane) for 1 H and 13 C or 1 N Al(NO 3 ) 3 aqueous solution for 27 Al nucleus …”

“…Chemical shifts were externally calibrated with respect to TMS (tetramethysilane) for 1 H and 13 C or 1 N Al(NO 3 ) 3 aqueous solution for 27 Al nucleus. 15 2.4. Ion Exchange of OSDAs into Various FAU Materials.…”