“…This was placed in the freezer (-30 • C) to give 4 as an olive-green microcrystalline solid, which was isolated by filtration, washed with 2 ¥ 3 mL n-pentane and dried under vacuum. Yield: 42 mg (34% 102.68, 103.02, 103.49, 114.68, 115.33, 116.52, 122.11, 122.37, 122.55, 124.33, 128.03, 128.46, 128.71 (appears in the DEPT-135), 129.62, 130.33, 130.44, 130.59, 132.31, 140.88, 142.33, 142.81, 153.53, 154.50, 155.19 (aromatics), 320.3 (detected indirectly by a gc2hsqcse experiment, [Ru]=C(H)Ph) (the ipso carbon in [Ru]=C(H)C 6 H 5 could not be located); 31 10b were charged in a Schlenk tube. This was connected to a Schlenk line and DCM (approx.…”