On the Determination of Mercury

Yoshida, Yukito

doi:10.1246/nikkashi1921.60.1124

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Synthesis and Characterization Of Compounds 1-201

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2009

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“…Compound 1 and 8 are reported to be synthesized by reacting Ti(OBu) 4 with the corresponding phenol. [58] The reported procedure for 3, [59] 9 [60] and 13 [61] is the direct reaction of titanium halide with the appropriate phenol. Compound 11, was synthesized using the reported procedure.…”

Section: Synthesis and Characterization Of Compounds 1-20mentioning

confidence: 99%

New Aryloxy and Benzyloxy Derivatives of Titanium as Catalysts for Bulk Ring‐Opening Polymerization of ϵ‐Caprolactone and δ‐Valerolactone

2009

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A variety of aryloxy compounds and benzyloxy derivatives of Ti IV were synthesized from Ti(iPrO) 4 using the alcoholysis route. These compounds were characterized using various analytical methods and single-crystal X-ray diffraction. Multinuclear NMR studies prove high degree of fluxional behavior of these compounds in solution. They adopt a dimeric structure in the solid state as seen from X-ray diffraction studies on a few of them. These compounds are powerful catalysts for the ring-opening polymerization of ε-caprolactone (CL) and δ-valerolactone (VL) resulting in high polymers with good number average molecular weights (M n ). Signifi-

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Section: Synthesis and Characterization Of Compounds 1-20mentioning

confidence: 99%