“…Successive impacts between milling balls and powder result in the formation of a large amount of point defects together with the fragmentation, amorphization and dissolution of the alloyed components (Y 2 O 3 and TiH 2 ) [6][7][8][9][10]. MA is therefore an out of equilibrium process and is known to form solid solutions of immiscible materials [11][12][13][14]. Numerous milling parameters are involved in mechanical alloying as the milling atmosphere, time and intensity, the mill type or different type of contaminations (powder or gas purity, milling balls, powder transfers).…”