2024
DOI: 10.1021/acs.joc.3c02605
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O–H Insertion of Hydrogenphosphate Derivatives and α-Diazo Compounds

Fei Tan,
Wei Wang,
Xiao Huang
et al.

Abstract: An efficient O−H insertion of hydrogenphosphate derivatives and α-diazo compounds has been developed to construct α-phosphoryloxy scaffolds. Diverse α-phosphoryloxy skeletons could be obtained under mild and catalyst-free conditions in good yields. The control experiments suggest a protonation and nucleophilic addition process of α-diazo compounds via a diazonium ion pair for this transformation.

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