Notes- A Preparation of 10-Hydroxydecanoic Acid

Benton, F. L.; Kiess, A. A.

doi:10.1021/jo01073a616

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Cited by 14 publications

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“…Lactones C 7 , C 8 , and C 12 were prepared from the corresponding ketones through Baeyer−Villiger oxidation . Methyl 10-hydroxydecanoate was prepared from methyl 11- undecenoate . Lactone C 11 was prepared from 11-bromoundecanoic acid .…”

Section: Methodsmentioning

confidence: 99%

Simple Preparation of Highly Pure Monomeric ω-Hydroxycarboxylic Acids

Stephan

Mohar

2006

Org. Process Res. Dev.

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Highly pure monomeric ω-hydroxycarboxylic acids (HCAs) with gC 6 are prepared from their corresponding lactones or alkyl ω-hydroxycarboxylates through saponification followed by H 2 SO 4 acidification and treatment at 35-40 °C/8-12 mbar or by freeze-drying. The HCA is being formed through its sodium or potassium salt and is obtained in 80-85% yield with >99.5% purity, uncontaminated with dimers. This simple procedure excludes chromatographic purification.

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Section: Methodsmentioning

confidence: 99%