“…The single crystals were obtained by recrystallization from dichloromethane. X-ray data from a monoclinic crystal (colorless block, 0.10×0.05×0.05 mm) were collected on a RIGAKU Saturn 724+ CCD device at 93 K. Crystallographic parameters are as follows: space group P2 1 /n, a = 9.097(7) Å, b = 11.824(11) Å, c = 10.128(10) Å, β = 106.64 (2) -3 , F(000) = 448.00. The intensities of 7652 reflections (multi-layered mirror monochromatic MoK α radiation, 2θ max = 52°, R int = 0.0418 for 2027 unique reflections (1652 for I > 2σ(I )), numerical absorption correction) were measured; R(I > 2σ(I), all data) = 0.0425, 0.0567, wR(I > 2σ(I ), all data) = 0.0926, 0.0996, GOOF on F 2 = 1.050, Δρ max = 0.23 e/Å -3 , Δρ min = -0.23 e/Å -3 , Data / restrains / parameters = 2027 / 0 / 146.…”