Nickel(II) Complexes of N,N'-Disubstituted Dithiooxamides<sup>1</sup>

Hurd, Richard N.; DeLaMater, George; McElheny, George C.; Peiffer, Leroy V.

doi:10.1021/ja01502a004

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S Reactions With Metal Ions1

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2014

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Cited by 33 publications

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“…The title compound, (I), is a representative of the relatively scarcely studied N-substituted thiooxamides, which may be used as versatile nitrogen-and sulfur-containing ligands for multinuclear metal complexes with special magnetic properties (Hurd et al, 1960). Only a few such molecules have been reported (Cui et al, 2004), because of the difficulties in their preparation and purification.…”

Section: Commentmentioning

confidence: 99%

N,N′-Bis[2-(diethylamino)ethyl]dithiooxalamide

et al. 2005

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Section: Commentmentioning

confidence: 99%

N,N′-Bis[2-(diethylamino)ethyl]dithiooxalamide

et al. 2005

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“…The title compound is a representative of the relatively scarcely studied N-substituted thiooxamides, which may be used as versatile nitrogen-and sulfur-containing ligands for multinuclear metal complexes with special magnetic properties (Hurd et al, 1960). Only a few such molecules have been reported (Cui et al, 2004), because of the difficulties in their preparation and purification.…”

Section: Commentmentioning

confidence: 99%

N,N′-Bis[2-(2-pyridyl)ethyl]dithiooxamide

et al. 2005

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The title compound, C16H18N4S2, has a crystallographic inversion centre at the mid‐point of the central C—C bond. The plane of the dithiooxamide fragment is approximately perpendicular to the plane of the dimethylene bridge [dihedral angle = 84.8 (1)°], the plane of which is in turn normal to the pyridine ring plane [dihedral angle = 89.80 (8)°]. An intermolecular N—H⋯N hydrogen bond involving the amide NH group and the pyridine N atom [N⋯N = 3.0503 (18) Å and N—H⋯N = 145.8 (14)°] links the molecules into chains extending along the c axis.

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“…N-coordinating-group substituted dithiooxamides can be used to synthesize multinuclear metal complexes with S and N as donor atoms (Hurd et al, 1960). A few studies on dinuclear or trinuclear metal complexes coordinated by dithiooxamide with substituents 2-aminomethylpyridine (Cui et al, 1999), 2aminoethylpyridine (Cui et al, 2004), amino acids (Veit et al, 1984;Castineiras et al, 2001) and 2-hydroxyethyl (Girerd et al, 1978) have been reported.…”

Section: Commentmentioning

confidence: 99%