New fluorogenic chemosensors derived from benzimidazole

Тихомирова, К. С.; Толпыгин, И. Е.; Starikov, А. G.; Kaz’mina, M. A.

doi:10.1007/s10593-017-2037-5

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Design Synthesis and Characterisation1

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“…Type II BZs were obtained by a two-steps procedure ( Scheme 2 ). BZ is 1 -5 were reacted with different aldehydes in the presence of glacial acetic acid to obtain the corresponding imines, which were then reduced with NaBH 4 to provide BZs 11 to 30 in 17 with a 57% yield [ 29 ]. Physicochemical, MS, NMR and IR spectral data for BZs type II are reported in the experimental Sections 4.1.2.8.1 -20 .…”

Section: Design Synthesis and Characterisationmentioning

confidence: 99%

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Further and new target-based benzimidazole anthelmintics active against Teladorsagia circumcincta

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Section: Design Synthesis and Characterisationmentioning

confidence: 99%

“…4.1.2.8. General procedure for the preparation of type II BZs 11 to 30[ 29 ]. To a solution of 0.75 mmol of each BZ i and the same proportion of the corresponding aldehyde in 10 mL of absolute EtOH, three drops of glacial acetic acid were added.…”

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confidence: 99%