Here in this paper we report a new series of 1,3,4-thiadiazole based heterocyclic monoazo dyes which have been derived by the diazotization of N 4 -(5-benzyl-1,3,4-thiadiazol-2-yl)-1,3-thiazole-2,4-diamine with various phenyl pyrazolone as coupling components. The structure of the synthesized dyes was characterized by elemental analysis, IR, 1 H NMR and UV spectroscopy with a view to determine their chemical structure. All the synthesized compounds were evaluated for their dyeing performance and fastness properties. The synthesized disperse dyes were found to possess very good dyeing properties.