Neutron Guinier camera

Abstract

The feasibility of Guinier cameras for small angle neutron scattering (SANS) is analyzed theoretically and experimentally. Small angle X-ray scattering (SAXS) is commonly measured with Guinier cameras 1 that use bent perfect crystals to focus to detector beams from point sources of characteristic X-rays. Neutron Guinier cameras do not exist yet, although focusing to detector has occasionally been tried. The philosophy of current SANS pinhole instruments is to gain intensity from broad wavelength bands at tight collimation. With characteristic X-rays, intensity gains can only come from broad angular divergences. Neutron focusing instruments represent a return, at a higher level, to the philosophy of characteristic X-rays. Such a return is advocated in this paper for SANS.The resolution of Guinier cameras is defined not by the collimation (which is relaxed), but by the beam size at focus and the spatial resolution of the position sensitive detector (which should match each other). Within the recent concept of neutron imaging 2 multi-wafer monochromators can provide image sizes comparable to the thickness of one wafer in the bent packet. The imaging may be non-dispersive, at broad wavelength bands, like with mirrors in conventional optics. These are the right ingredients for convergent neutron beams in Guinier cameras. The paper addresses the question whether the increased angular divergence can compensate for the reduced size of the source that is imaged into a sharp spot at detector.A neutron Guinier camera at thermal neutron energies is evaluated. It turns out to be quite feasible, providing moderate resolution at high intensity with detection systems in current use for high-resolution neutron diffraction. High-resolution SANS is also possible with detection systems of sub-millimeter spatial resolution.Tests were performed using a single wafer and a packet of bent silicon wafers in both Bragg and Laue (transmission) geometry in non-dispersive imaging arrangements. Experiments have confirmed expectations. SANS data obtained in neutron Guinier camera conditions on samples of collagen and lipids are presented.