“…RAFT is one of the most powerful and versatile controlled radical polymerization techniques [ 11 ] for the synthesis of complex multiblock architectures [ 12 , 13 , 14 , 15 , 16 , 17 , 18 ] as well as so-called “smart” materials, such as switchable filtration devices [ 19 , 20 , 21 ] or nanocarriers for biomedical applications [ 22 , 23 , 24 ]. Within this group of “smart” materials, especially upper critical solution temperature polymers, such as this work’s optimization target polymethacrylamide (PMAAm) [ 25 , 26 ], have received increasing attention [ 27 , 28 , 29 , 30 ].…”