1Introduction dation potential was higher,i na greementw ith TP structure. Formalp otentials in aqueous solutions that have been previouslyu navailable from electrochemistry of CA and TP were thus obtained. In the determinations of CA and TP,s ensitivity and linear dynamic range (LDR)i n FSV were 1.84 mA cm À2 mM À1 and 0.20-22.0 mmol L À1 and 1.46 mA cm À2 mM À1 and 0.50-30.0 mmol L À1 ,r espectively. FSV determination of CA in coffee sample is demonstrated and the results are in agreement with the results obtained by HPLC-UV.