Abstract:diquinoline 8 forms clathrate compounds on crystallization from benzene, acetone, or diethyl ether. Their crystal structures are analyzed in crystal engineering terms. Molecules of 8 form robust dimers, containing swivel angles around 110°, and assembled through a combination of seven intermolecular attractions. Two enantiomeric dimers assemble around an inversion center by means of eight further attractions. A cyclic R 2 2 (8) motif utilizing −CBr−H•••N weak hydrogen bonds is the key construction element used… Show more
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