Abstract:Hexagonal 1D AlN whiskers were synthesized by direct nitridation of aluminum and alumina. The effect of the atmosphere was investigated based on thermodynamic calculation. A green body compacting alumina with different particle size in between 44–420 μm in graphite crucible was found to be favorable for the large-scale synthesis of AlN at 1650 °C for 3 h in flowing nitrogen atmosphere. XRD result indicated that hexagonal AlN phase with high purity has been successfully synthesized. SEM and TEM analysis indicat… Show more
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