This report documents work performed under the Spent Fuel and Waste Disposition's Spent Fuel and Waste Science and Technology program for the US Department of Energy (DOE) Office of Nuclear Energy (NE). This work was performed to fulfill Level 2 Milestone M2SF-21OR010201032, "ORNL High Burnup Confirmatory Demo Sibling Rod Testing Results," within work package SF-21OR01020103 and is an update to the work reported in M2SF-19ORO010201026 and M2SF-19OR010201028. As a part of DOE NE High Burnup Spent Fuel Data Project, Oak Ridge National Laboratory (ORNL) is performing destructive examinations (DEs) of high burnup (HBU) (>45 GWd/MTU) spent nuclear fuel (SNF) rods from the North Anna Nuclear Power Station operated by Dominion Energy. The SNF rods, called sister rods or sibling rods, are all HBU and include four different kinds of fuel rod cladding: standard Zircaloy-4 (Zirc-4), low-tin (LT) Zirc-4, ZIRLO, and M5. The DEs are being conducted to obtain a baseline of the HBU rod's condition before dry storage and are focused on understanding overall SNF rod strength and durability. Composite fuel and defueled cladding will be tested to derive material properties. Although the data generated can be used for multiple purposes, one primary goal for obtaining the post-irradiation examination data and the associated measured mechanical properties is to support SNF dry storage licensing and relicensing activities by (1) addressing identified knowledge gaps and (2) enhancing the technical basis for post-storage transportation, handling, and subsequent disposition. This report documents the status of the ORNL Phase 1 DEs of eight sister rods and outlines the DE tasks performed and the data collected to date, as guided by the sister rod test plans. The DEs are performed using a phased approach, and the Phase 1 DEs being performed at ORNL include: • full-length rod heat treatments (FHT) of three selected sister rods to examine the effects of temperatures reached during dry storage preparation; Sister Rod Destructive Examinations November 30, 2020 v Planned DE Status Comments measurement uncertainty of the baseline rod, and the heat-treatment did not appear to affect the void volume. No conclusions could be made about the effects of the heat-treatment on the Zirc-4-clad rod based on a comparison with the LT Zirc-4 baseline rod or the Pacific Northwest National Laboratory Zirc-4-clad rod. Comparisons with predictions from fuel rod performance codes FAST and BISON indicate a tendency for FAST to overpredict void volume and BISON to underpredict void volume. Measure the transmissibility of gas along the pellet stack Complete Pellet stack gas transmissibility at room temperature was measured by using depressurization tests on eight rods and transmission tests on three rods. In all cases, gas was transmissible through the pellet stack at room temperature, requiring between 30 min and 24 h to reach equilibrium conditions, depending upon the pressure differential applied. The data correlates well using the Muskat-Poiseuille porous media me...