Drying of Porous Materials
DOI: 10.1007/978-1-4020-5480-8_16
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Modeling of vacuum desorption of multicomponent moisture in freeze drying

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Cited by 3 publications
(3 citation statements)
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“…This drying process is conventionally divided into three stages: pre-freezing of wet material, primary drying stage (sublimation of frozen solvent under vacuum), and secondary drying stage (desorption of residual bound water from material matrix) (Nastaj and Ambrożek, 2006;Nastaj and Witkiewicz, 2009). To improve storage stability of dried products, residual water after the primary drying stage may further be removed by desorption in the secondary drying stage (Nam and Song, 2007).…”
Section: Freeze Drying (Fd)mentioning
confidence: 99%
“…This drying process is conventionally divided into three stages: pre-freezing of wet material, primary drying stage (sublimation of frozen solvent under vacuum), and secondary drying stage (desorption of residual bound water from material matrix) (Nastaj and Ambrożek, 2006;Nastaj and Witkiewicz, 2009). To improve storage stability of dried products, residual water after the primary drying stage may further be removed by desorption in the secondary drying stage (Nam and Song, 2007).…”
Section: Freeze Drying (Fd)mentioning
confidence: 99%
“…1. Microwave-assisted freeze drying is a multiple-stage operation usually performed at three stages: prefreezing of the wet material, the primary drying stage when direct sublimation of the frozen water takes place under vacuum and secondary drying stage when residual bound water is desorbed from the material matrix (Nastaj & Ambrozek, 2007;Nastaj & Witkiewicz, 2009). The time that secondary drying stage takes to remove the sorbed water can be as long as or longer than the time that is required for the removal of the free water (Jiang et al, 2010c).…”
Section: Resultsmentioning
confidence: 99%
“…This is one of the major reasons why this technique has been developed in laboratory in the past several decades but not applied in practice at present. Like FD, MFD is a multiple-stage operation usually performed at three stages: pre-freezing of the wet material, the primary drying stage when direct sublimation of the frozen water takes place under vacuum, and secondary drying stage when residual bound water is desorbed from the material matrix (Nastaj and Witkiewicz, 2009;Nastaj and Ambrozek, 2007). At each stage some changes occur in starch content, reducing sugar content, the porosity of internal structure and color, some of which can cause quality deterioration during MFD.…”
Section: Introductionmentioning
confidence: 99%