“…Specially designed batch cells (sample volume $0.8 mL) made from stainless steel with a perfluoroelastomer O-ring seal (Kalrez 4079) were used. A discontinuous step method was employed with heating/cooling rates of 0.1 K/min and an isothermal delay of 3600 s [8,9]. The power difference needed to heat or cool the reference and sample cells between (297.65 and 298.65) K (1 K step) were determined by integration of the heat flow signals.…”
“…Specially designed batch cells (sample volume $0.8 mL) made from stainless steel with a perfluoroelastomer O-ring seal (Kalrez 4079) were used. A discontinuous step method was employed with heating/cooling rates of 0.1 K/min and an isothermal delay of 3600 s [8,9]. The power difference needed to heat or cool the reference and sample cells between (297.65 and 298.65) K (1 K step) were determined by integration of the heat flow signals.…”
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