2011
DOI: 10.1016/s1003-6326(11)60995-3
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Microstructure evolution of a new directionally solidified Ni-based superalloy after long-term aging at 950 °C upto 1 000 h

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Cited by 10 publications
(5 citation statements)
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“…In addition to these nucleated precipitates, several cavities were generated in the aged blades heterogeneous microstructure after 55,000 EOH at 870°C mixed with aligned γ′ phase as shown in Figure 5(b), provide evidence of the entrance in tertiary creep phase that can provoke buckets failure. Another life-limiting phenomenon mainly observed in aged buckets nickel-based superalloys at 870°C, was the transformation exhibited in Figure 6, of large blocky MC-Carbides rich in (Ti, Ta) found in γ-matrix into coarse brittle Cr rich M 23 C 6 lines network at the grain boundaries of GTD-111 base material [19,20]. On another side, the cold air circulated during service inside the buckets internal channels, had reacted directly with blades base metal and formed an accumulated thick layer of (Al 2 O 3 , TiO, C 2 O 3 , Er 2 O 3 , SiO 2 ) mixed oxides scales (as shown in Figure 7).…”
Section: Discussionmentioning
confidence: 99%
“…In addition to these nucleated precipitates, several cavities were generated in the aged blades heterogeneous microstructure after 55,000 EOH at 870°C mixed with aligned γ′ phase as shown in Figure 5(b), provide evidence of the entrance in tertiary creep phase that can provoke buckets failure. Another life-limiting phenomenon mainly observed in aged buckets nickel-based superalloys at 870°C, was the transformation exhibited in Figure 6, of large blocky MC-Carbides rich in (Ti, Ta) found in γ-matrix into coarse brittle Cr rich M 23 C 6 lines network at the grain boundaries of GTD-111 base material [19,20]. On another side, the cold air circulated during service inside the buckets internal channels, had reacted directly with blades base metal and formed an accumulated thick layer of (Al 2 O 3 , TiO, C 2 O 3 , Er 2 O 3 , SiO 2 ) mixed oxides scales (as shown in Figure 7).…”
Section: Discussionmentioning
confidence: 99%
“…The precipitation and growth kinetics of the γ' phase are highly sensitive to the rate at which the alloy is cooled through the solvus temperature. The (γ+γ') eutectic is an indication of the remaining melt at the end of the solidification process [7,8]. After solution heat treatment, the microstructure with (γ+γ') eutectic should be homogenized [9].…”
Section: Materialmentioning
confidence: 99%
“…The alkali fusion method has the shortcomings of high alkali consumption, complex processing, and a large amount of waste residue, while the acid method of extracting Al 2 O 3 from coal gangue has the advantages of high efficiency and simplicity. Guan et al , 18 extracted Al 2 O 3 directly under a hydrochloric acid system by adding sodium fluoride, and the extraction ratio of Al 2 O 3 only reached only 70.40%. The structures of kaolinite, muscovite, and orthoclase within coal gangue are stable, and hydrochloric acid is not reactive and cannot efficiently extract Al 2 O 3 .…”
Section: Introductionmentioning
confidence: 99%