The recrystallisation behaviour of IN 718 has been analysed using a Gleeble 1500 thermomechanical simulator. The use of a rapid water quenching system immediately after the compression test has resulted in the ability to separate dynamic behaviour from meta-dynamic. The rate of dynamic recrystallisation has been found to be proportional to temperature and strain, but inversely proportional to strain rate. The nucleation rate of recrystallised grains during deformation has been found to be directly linked to strain rate and temperature. The rate of meta-dynamic recrystallisation appears to be directly proportional to temperature and strain rate, but no new nucleation events were observed after the end of deformation
MethodsMaterial was supplied for the experiments by Firth Rixson Forgings Ltd in the form of a forged and rolled billet of IN 718. Cylindrical samples of height 12 mm and diameter 8 mm were spark eroded from the billet and deformed using a Gleeble 1500 thermomechanical simulator.Initially, the effects of temperature and strain rate on dynamic recrystallisation were investigated. Samples were deformed at a temperature of either 980 • C or 1040 • C to predefined strains of 0·09, 0·18, 0·29, 0·41, 0·53, 0·67, and 0·82 at a set die velocity resulting in average strain rates of 0·01, 0·1, 0·45, and 1·1 s −1 followed by an immediate water quench. To investigate meta-dynamic recrystallisation, samples deformed to a strain of 0·82 were also held at the test temperature for times ranging from 1 second to 10 minutes before undergoing a water quench. Each experiment begins with a linear heat-up to test temperature over 2 minutes and then a hold for 1 minute. The tests were followed by a water quench designed to reduce the temperature of the sample as quickly as possible. Figure 1 shows the temperature profile of a typical test, showing the heat-up, hold, and quench. Thermal data is plotted for both the centre of the sample, and either end, measured using thermocouples welded to the sample. It can be seen that, although a large thermal gradient exists during the heating stage, after a 1 minute hold period, the sample is at a uniform temperature. Referring to Figure 1 (b), it can be seen that the water quench stage lowers the temperature of the specimen extremely rapidly. It takes only 1·1 seconds for the sample to reach 200 • C, and less than 0·2 seconds for the centre of the sample to fall below 800 • C (a temperature below which the rate of recrystallisation is almost zero).