1985
DOI: 10.1021/ed062p147
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Microscale organic laboratory: I: An approach to improving air quality in instructional laboratories

Abstract: Increased awareness of the significance of low gas phase concentrations of commonly used chemicals in instructional laboratories has been reflected in previous articles on lab safety (1-4).In moving toward cleaner laboratory air, it is likely that many institutions have been guided by the occupational exposure standards established by the Occupational Safety and Health Administration (5). In one case (4), an institution has adopted as policy the maintenance of air quality based on the Permissible Exposure Leve… Show more

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Cited by 4 publications
(4 citation statements)
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“…Como reconocen los protagonistas surgió, al menos en parte, para dar solución al problema de renovación, a un coste asequible, de un laboratorio de Química Orgánica obsoleto que no cumplía con la reglamentación vigente. Las técnicas y materiales necesarios fueron desarrollados en 1982, los primeros resultados se dieron a conocer en 1984 (Pike et al, 1984;Butcher et al, 1984) y fueron publicados el año siguiente (Butcher et al, 1985;Mayo et al, 1985).…”
Section: De Aniversariounclassified
“…Como reconocen los protagonistas surgió, al menos en parte, para dar solución al problema de renovación, a un coste asequible, de un laboratorio de Química Orgánica obsoleto que no cumplía con la reglamentación vigente. Las técnicas y materiales necesarios fueron desarrollados en 1982, los primeros resultados se dieron a conocer en 1984 (Pike et al, 1984;Butcher et al, 1984) y fueron publicados el año siguiente (Butcher et al, 1985;Mayo et al, 1985).…”
Section: De Aniversariounclassified
“…Since Mayo et al first performed microscale organic synthesis with reagent consumption at the mmol level in the 1980s, the past several decades have witnessed the widespread application of microscale chemistry experiments (MCEs) in chemical education at universities and high schools. MCEs are experiments that consume minimal amounts of reagents in miniaturized instruments while still providing the required chemical information. MCEs are more cost-effective and environmentally friendly than conventional chemistry experiments, owing to reduced reagent consumption and waste production.…”
Section: Introductionmentioning
confidence: 99%
“…Microscale technique, also known as small scale technique, is an environmentally viable option for conducting chemical processes through laboratory experiments using small quantities of starting materials without compromising the quality and standard of chemical applications in education and the industry. In this sense, students who used to work with 10-50 g of reactants and 50-500 g of solvent may now work with only about 10-150 mg of starting materials and 1-10 g of solvent (Buther et al, 1985).…”
Section: Introductionmentioning
confidence: 99%