“…The students can then be readily taught the limitations and advantages of each of these methods. Among the sulfur methods we mention in passing the industrial titration of SOy" by means of the tetrahydroxyquinone indicator and the technic of using a color filter to determine a difficult endpoint (13).…”
“…The students can then be readily taught the limitations and advantages of each of these methods. Among the sulfur methods we mention in passing the industrial titration of SOy" by means of the tetrahydroxyquinone indicator and the technic of using a color filter to determine a difficult endpoint (13).…”
“…(10) Kulikov, I. V., and Panova, S. V., J. Gen. Chem. (U. S. S. R.), 2 (64), 736 (1932). Presented before the Division of Analytical and Micro Chemistry at the 102nd Meeting of the American Chemical Society, Atlantic City, N. J.…”
“…Hallett and Kuipers (2), Sundberg and Royer (6), Alieino (1), and Ogg, Willits, and Cooper (4). All these authors used the catalytic combustion method to destroy organic material and to convert the organically bound sulfur to sulfate, previous to the titration with barium chloride.. A demonstration by Willits and Ogg in their laboratory convinced the present authors of the value of the illuminated titration stand technique, and they decided to adopt the method in this laboratory.…”
A micromethod for determining sulfur is presented which employs the Carius combustion followed by titration of the resulting sulfate with barium chloride. The tetrahydroxyquinone indicator method of Ogg, Willits, and Cooper is used. HE use of the tetrahydroxyquinone indicator (prepared by W.
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