2009
DOI: 10.1002/adv.20162
|View full text |Cite
|
Sign up to set email alerts
|

Method to describe curing in large epoxy samples

Abstract: ABSTRACT:Curing kinetics models used in numerical simulations describe the exothermic chemical reaction of thermosetting materials. The mathematical formula known as Kamal's model is discussed in the following paper. Traditionally, the coefficients of Kamal's equations are estimated based on differential scanning calorimetry (DSC) measurements and results from an experimental verification of such created curing kinetics model are presented. Furthermore, an inverse analysis is proposed for additional adjustment… Show more

Help me understand this report

Search citation statements

Order By: Relevance

Paper Sections

Select...
1
1
1
1

Citation Types

0
6
0

Year Published

2012
2012
2021
2021

Publication Types

Select...
5

Relationship

1
4

Authors

Journals

citations
Cited by 6 publications
(7 citation statements)
references
References 5 publications
0
6
0
Order By: Relevance
“…Optimum value as in (12) and constraints in (13) were set in order to obtain an optimum cycle; that is, reaction peak did not exceed 132 ∘ C and the total cycle time was set to a minimum, not exceeding 9 minutes and comprising a onestep cycle time as shown in Figure 10:…”
Section: Reaction Peak Temperature and Cycle Time Reductionmentioning
confidence: 99%
See 1 more Smart Citation
“…Optimum value as in (12) and constraints in (13) were set in order to obtain an optimum cycle; that is, reaction peak did not exceed 132 ∘ C and the total cycle time was set to a minimum, not exceeding 9 minutes and comprising a onestep cycle time as shown in Figure 10:…”
Section: Reaction Peak Temperature and Cycle Time Reductionmentioning
confidence: 99%
“…They carried out simulation considering the heat conductivity and heat capacity changes during cure process and raised the accuracy of estimation by comparing the results with those by experiments. Kasza et al [13] improved the accuracy of estimation in the cure kinetics model by considering a buoyancy flow during liquid phase and by carrying out a sensitivity analysis for a large epoxy sample having axis-symmetry. Liu et al [14] performed threedimensional finite element analysis by proposing a chemothermo-microwave curing model for the microwave cure epoxy in the flip chip packaging process.…”
Section: Introductionmentioning
confidence: 99%
“…This is governed by the importance of allowing for the structural factor in planning the synthesis of the polymer material, and also in assessing its mechanical and service properties [5]. A shortcoming of existing kinetic models of curing is the laboriousness of calculations and the need to use additional kinetic approaches to finding the coefficients in the equations [6]. We set ourselves the task of a theoretical description of the formation of a densely crosslinked polymer system, taking into account non-linear factors in the dynamics of change in its configuration during synthesis.…”
Section: Selected From International Polymermentioning
confidence: 99%
“…In turn, in isothermal DSC several experimental runs are performed and the sample temperature is kept constant at different levels (e.g., 100, 120, or 140 • C) during each such run. 9 In both DSC methods, the heat flow into or from a sample is recorded as depicted in Fig. 5.…”
Section: Calorimetric Experimentsmentioning
confidence: 99%
“…In dynamic DSC, the sample is usually heated starting from ambient conditions with different heating rates, for example, 2, 5, or 10 K/min. In turn, in isothermal DSC several experimental runs are performed and the sample temperature is kept constant at different levels (e.g., 100, 120, or 140°C) during each such run 9. In both DSC methods, the heat flow into or from a sample is recorded as depicted in Fig.…”
Section: Rheological Pressure and Calorimetric Measurementsmentioning
confidence: 99%