Metallic amorphous electrodeposited molybdenum coating from aqueous electrolyte: Structural, electrical and morphological properties under current density

Efficient Electrochemical N2 Reduction to NH3 on MoN Nanosheets Array under Ambient Conditions

“…XPS and EDX spectra suggest the absence of N in MoN after electrolysis under Ar atmosphere (Figure S11 and S12a) while the maintaince of N in MoN under N 2 atmosphere (Figure S6 and S12b). The XRD pattern (Figure S13) indicates the formation of metallic Mo after long-term electrolysis under Ar . We performed a 15 N isotopic labeling experiment to verify the N source of the produced NH 3 .…”

“…The XRD pattern (Figure S13) indicates the formation of metallic Mo after longterm electrolysis under Ar. 36 We performed a 15 N isotopic labeling experiment to verify the N source of the produced NH 3 . As shown in Figure S14, 1 H nuclear magnetic resonance spectra ( 1 H NMR) show a triplet coupling for 14 NH 4 + and a doublet coupling for 15 .…”

Electrodeposition and the Optimization of Molybdenum Layer on Nb-Ti-Si Based Ultra-High Alloys from Aqueous Solution

“…Adopting the same method, Syed [19] deposited thicker (≈20 μm) and metallic molybdenum layer on mirror polished Cu substrate from aqueous water and gave plausible mechanism of the reduction. Nemla [20] investigated the structural electrical and morphological properties of the as-deposited amorphous molybdenum coating under different current density respectively.…”