“…The resulting precipitate was collected by filtration, washed with water and recrystallized in ethanol. [24] White solid; mp 189-191 °C; yield 94 %; IR (KBr, cm À 1 ): 3100-2900 (CÀ H), 1640 (C=O), 1510 (C=N), 1420 (C=C); 1 H NMR (500 MHz, CDCl 3 ) δ 10.05 (s, 1H), 9.74 (dd, J = 2.1, 0.8 Hz, 1H), 7.74 (dd, J = 9.5, 0.8 Hz, 1H), 7.69 (m, 2H), 7.68 (m, 2H), 7.56 (dd, J = 9.4, 2.0 Hz, 1H); 13 C NMR (126 MHz, CDCl 3 ) δ 179. 36, 157.16, 146.15, 132.40, 131.93, 131.15, 127.00, 124.97, 123.92, 120.92, 117.83; m/z 335.95.…”