This research was based on influence of various fly ash filler content in the machining properties of Pineapple (P)/Sisal (S) hybrid fiber reinforcement composites. Fly ash from bio waste materials of Bagasse (BGFA), Banana (BFA) and Coir (CFA) were used. High hardness nature of 3% BFA (22.73 HV) and 3% CFA (23.85 HV) reduces Material Removal Rate (MRR) and increases its surface roughness nature of the composites. Maximum MRR of 376.38 mm 3 min −1 was observed in 3% BGFA combinations with 250 MPa Water jet Pressure (WP), 1mm Standoff Distance (SOD) and 20 mm min −1 Traverse Speed (TS) as machining parameters. MRR of 353.64 and 352.76 mm 3 min −1 was found out with 1% CFA and 1% BFA combinations. Lower surface roughness of 6.39 μm, 6.71 μm and 6.75 μm was found in 3% BGFA, 1% CFA and 1% BFA based composites. Filler surface created a tight bonding with the matrix, which reduces the erosion of fiber particles at higher WP. Untreated fibers showed lesser machining properties due to low fiber/matrix bonding. SEM results showed reducing of cracks and matrix breakages by the substitution of filler powders.