Mechanochemical Synthesis and Three-Dimensional Electron Diffraction Structure Solution of a Novel Cu-Based Protocatechuate Metal–Organic Framework
Andrea Sala,
Moussa D. Faye Diouf,
Danilo Marchetti
et al.
Abstract:Mechanochemical synthesis is a powerful approach to obtain new materials, limiting costs, and times. However, defected and submicrometrical-sized crystal products make critical their characterization through classical single-crystal X-ray diffraction. A valid alternative is represented by three-dimensional (3D) electron diffraction, in which a transmission electron microscope is used, like a diffractometer. This work matches a green waterbased mechanochemical synthesis and 3D electron diffraction to obtain and… Show more
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