Friction stir welding is a solid-state method of joining thermoplastic materials. This paper studied the effect that varying process parameters (rotational speed, welding speed, and attack angle) had on the weld quality of polyethylene sheets. Experiments were performed at rotational speeds of 1000, 1200, 1400, 1600, and 1800 r/min, welding speeds of 12, 16, and 20 mm/min, and attack angles of 1˚and 2˚. A strength value of 75 per cent of that of the base material was achieved at the isolated optimum welding condition. Changes in the weld zone microstructure were investigated using differential scanning calorimetry and scanning electron microscopy. The observed microstructures were used to explain the reduced value of the strength.