“…4 Utilized since the 1930s, 5 reaching a peak in research in the 1980s, 3,[6][7][8][9] it is currently applied in a vast array of research disciplines, 10 including the billion dollar nanomaterials industry. 4,11,12 Acid-catalyzed silica solgel processes are used, e.g., to produce xerogels, which find applications in high-temperature ceramics, thermally isolating coatings, molecular filtration, and thin film sensors. 4,10,13 It has been stated that "a critical hurdle in the development of sol-gel techniques for the preparation of inorganic materials is elucidating the effect of key synthesis and processing parameters on the structure of the resulting sols".…”