Phone: þ90 312 203 34 52, Fax: þ90 312 212 73 43 A nanostructured NdMn 2 Ge 2 sample is prepared by a highenergy ball-milling technique. The structural and magnetic properties of ball-milled nanopowder have been studied by high-resolution transmission electron microscopy (HRTEM), atomic force microscopy (AFM), magnetic force microscopy (MFM), and magnetization measurements. According to the HRTEM results, the particle size of the nanoparticles changes from 5 to 11 nm. Curie and spin-reorientation temperatures are found to be 328 and 208 K from the temperature-dependent magnetization measurements, respectively. The maximum magnetic entropy change values are about À0.4 and À1.10 J kg À1 K À1 for DH ¼ 2T around the spin-reorientation (T SR ) and Curie (T C ) temperatures, respectively.