New K/Ar mineral ages of thirty nine samples (biotite, muscovite, K-feldspar) from the two-mica granodiorite to granite and leucogranite of the northern part of the Sithonia Plutonic Complex (Chalkidiki, Greece) are given in the present study. These data along with existing Rb/Sr mica and U/Pb zircon ages are used to investigate the thermal history of the plutonic complex and shed light on the process that affected it, and caused discordant Rb/Sr and K/Ar mineral ages. The K/Ar mineral dating yielded ages ranging from 38 to 49 Ma for muscovites, 32 to 47 Ma for biotites and 37 to 43 Ma for K-feldspars, respectively. The comparison of the K/Ar, Rb/Sr and U/Pb mineral ages and the closure temperatures of the different isotopic systems for the different minerals indicate a rapid cooling rate for the Sithonia pluton. The latter supports the hypothesis that the pluton was formed in a post orogenic extensional regime. Moreover, the K/Ar mineral isochrones indicate that a reheating of the pluton took place before 37 Ma and partially rejuvenated the K/Ar and Rb/Sr isotopic system of the minerals. to the lower closure temperatures of the minerals for the K/Ar isotopic system in respect to the Rb/Sr system, the former is more easily affected by any reheating and so it is more possible to detect any isotopic disturbance. The subject of the present study is the K/Ar mineral geochronology of the northern part of the Sithonia pluton. The systematic K/Ar study of the pluton in association with the previous geochronological studies sheds light on the pluton's thermal history after its emplacement and on its affinity with the geotectonic regime.
Analytical methodsThe samples were crushed and the 150-250 µm grain size was collected. A vibrating table and a Franz Isodynamic Magnetic separator (model L-1) were used to separate muscovite and biotite. K-feldspar was extracted using the same magnetic separator and the heavy liquid tetrabromoethane (Br 2 CHCHBr 2 ). The separation of the minerals was performed at the Department of Mineralogy, Petrology and Economic Geology, Aristotle University of Thessaloniki, Greece. Muscovite and biotite chemical analyses were performed on a JEOL scanning electron microscope at the Department of Mineralogy, Petrology and Economic Geology, Aristotle University of Thessaloniki, Greece. The operating conditions were: 20 kV and 20 nA, with a beam diameter < 1 mm.X-Ray Powder Diffraction analyses (XRPD) were performed on each mineral extract to calculate the proportion of mineral and the purity of it. Powder XRPD analyses were obtained on a PHILIPS PW1820/00 X-ray diffractometer of the Department of Mineralogy, Petrology and Economic Geology, School of Geology, Aristotle University of Thessaloniki, carrying a PW1710 microprocessor. The operating conditions for all samples were 35 kV and 25 mA using Ni-filtered CuK radiation. The 2-theta scanning range was between 3°a nd 63° and the scanning speed was 1.2 °/min. Refinements were done with the PCAPD software and the identification of the samples ...