We present fiber Bragg grating pressure sensors in air-hole microstructured fibers for high-temperature operation above 800°C. An ultrafast laser was used to inscribe Type II grating in two-hole optical fibers. The fiber Bragg grating resonance wavelength shift and peak splits were studied as a function of external hydrostatic pressure from 15 psi to 2000 psi. The grating pressure sensor shows stable and reproducible operation above 800°C. We demonstrate a multiplexible pressure sensor technology for a high-temperature environment using a single fiber and a single-fiber feedthrough. © 2010 Optical Society of America OCIS codes: 060.2370, 060.4005, 120.5475, 120.6780. Pressure sensors operated at high temperature above 500°C have many important applications in the energy industry. They ensure safe and efficient energy production during operations of gas turbines, coal boilers, nuclear power plants, and others. The hightemperature environment presents unique challenges to sensing systems. It not only requires robust sensor elements but also demands reliable packaging and wiring techniques rated for high-temperature environments.Fiber-based optical sensors have been considered good candidates for applications within harsh environments. For example, high-temperature pressure sensors based on a Fabry-Perot interferometer (FPI) have been successfully demonstrated [1,2], and fiber pressure sensors with operating temperatures up to 800°C have been achieved using sapphire fibers [1]. On the other hand, conventional fiber Bragg grating (FBG) sensors are generally considered unsuitable for high-temperature operation. Although FBG pressure sensors have been fabricated using UV laser writing, their operational temperature was limited to below 300°C owing to the poor thermal stability of the UV-induced refractive index change [3,4].In contrast to interferometer-based fiber sensors, FBG-based sensors are readily multiplexible, and the fabrication and the packaging of FBG sensors are relatively simple. They can be produced reliably and in large quantities using a phase mask writing technique. These highly desirable advantages have resulted in significant efforts to improve the hightemperature stability of FBG sensors. In particular, the adaptation of novel fibers, such as nitrogen-doped fiber [5], or novel fabrication techniques, such as ultrafast laser writings [6], has potentially improved the operational temperature of fiber grating devices to be on par with FPI-based sensors, approaching or exceeding 800°C.In this Letter, we apply femtosecond-pulsed ultrafast laser writing to produce high-temperature stable FBG in two-hole fibers for pressure sensing. This work demonstrates a significant improvement of the operational temperature of FBG pressure sensors in air-hole microstructured fiber to over 800°C. A large number of high-temperature FBG pressure sensors in microstructured fibers can be fabricated in one fiber using a simple phase mask approach. The multiplexed fiber sensor array in a single fiber can be serviced by...