Local structure analysis of short-lived reaction intermediates by means of a time-resolved stopped-flow extended X-ray absorption fine-structure technique.

Inada, Yuji

doi:10.2116/bunsekikagaku.49.563

Bunseki kagaku

2000

DOI: 10.2116/bunsekikagaku.49.563

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Local structure analysis of short-lived reaction intermediates by means of a time-resolved stopped-flow extended X-ray absorption fine-structure technique.

Yuji Inada

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2002

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Following the formation of nanometer-sized clusters by time-resolved SAXS and EXAFS techniques

et al. 2002

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Time-resolved in situ SAXS and XAS measurements were carried out to monitor the formation of nanoparticles of the sulfides of cadmium and zinc, from solutions containing he corresponding acetate, and thioacetamide under solvothermal conditions. Analysis of the SAXS data shows that particles of ca 5 nm in radius form within the first few minutes of the reaction and then grow uniformly to ca 20 nm over a period of two hours resulting in a highly mono-dispersed particle distribution. EXAFS data of the CdS particles also prepared by solvothermal methods and recorded at 20 K, support the formation of nano-meter sized particles.

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Following the formation of nanometer-sized clusters by time-resolved SAXS and EXAFS techniques

et al. 2002

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Local structure analysis of short-lived reaction intermediates by means of a time-resolved stopped-flow extended X-ray absorption fine-structure technique.

Cited by 1 publication

References 21 publications

Following the formation of nanometer-sized clusters by time-resolved SAXS and EXAFS techniques

Following the formation of nanometer-sized clusters by time-resolved SAXS and EXAFS techniques

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