Structure defects may be detected by all the non-destructive analysis techniques from radiography, magnetic particles, liquid penetrating, to ultrasounds, to eddy currents, etc. Nevertheless, to evaluate the quantity of liquid or gas that may be lost in the surrounding ambient specific techniques related to leak detection should be considered. Frequently the maximum acceptable leaks must be evaluated to select the method suitable for the specified object and, finally, to compare the solutions on the basis of costs-benefit relationship. Various leak detection methods and related instrumentation are available (bubbles, ultrasound emission, radar, pressure/vacuum variation, thermal conductivity, halogens, radioisotopes, selective ion pumping, mass spectrometry). Before starting any type of leak testing, it is necessary to decide whether leaks have to be located or measured. Checking the tightness of an object or device implies the measurement of gas flow coming out from a defect or entering through it and reference devices should be provided by primary or accredited laboratories. After a short review of methods/instrumentation attention is given to the calibration of any kind of systems and methods to guarantee the validity of the whole test.
General Considerations on LeaksIt is not possible, to date, to have systems or components absolutely tight even if the technology had enormous developments (Fig. 1). Containers always have a leak, be it of gas or liquid from a high-pressure artefact whether entry of fluid in an object kept at low pressure (Fig. 2).And then, some components for the operation of which a degree of tightness has to be guaranteed should be subjected to a control apt to show any leakage due to material defect, faulty workmanship, non hermetic assembly, material degradation The tightness test is a non-destructive test and may be defined as "a test performed to verify compliance of materials or components to specified requirements, using techniques that do not damage the characteristics or working performances".Only in a very lucky situation, so very rarely, a leak is represented by a cylindrical channel, more often it is due to a tortuous small duct or may also occur through a permeation process.The leak usually is not deformable, so it has a constant value unless strong mechanical or thermal stress occurs through the walls of a container located between two environments kept at different pressures (Fig. 3). A real leak causes a change of the pressure in the container and it is through a "hole" on a wall connecting the interior of the container with the atmosphere. Even a virtual leak causes a change in pressure inside the considered volume, but it is caused by the evolution of gas or vapour within the system itself, such as desorption of gas from the material of the container or diffusion within the wall followed by emission inside the chamber.A tightness test implies, therefore, measuring the flow of gas (the amount of gas in time), that escapes from the defect or enters in. Over the years ...