Lattice Dynamics of [Ni(NH3)6] (ClO4)2, [Ni(NH3)6] (BF4)2, and [Ni(NH3)6] (PF6)2

Kulczycki, A.

doi:10.1002/pssb.2221030237

Physica Status Solidi (b)

1981

DOI: 10.1002/pssb.2221030237

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Lattice Dynamics of [Ni(NH₃)₆] (ClO₄)₂, [Ni(NH₃)₆] (BF₄)₂, and [Ni(NH₃)₆] (PF₆)₂

A. Kulczycki

Abstract: The lattice dynamics of crystalline [Ni(NH3)6] (ClO4)2, [Ni(NH3)6] (BF4)2, and [Ni(NH3)6] (PF6)2 is studied in the framework of the point charge model. Phonon frequencies, in six high‐symmetry directions, and elastic constants are calculated. Good agreement with the experimental data for Raman active frequencies is achieved.

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1H and19F magnetic resonance study on molecular dynamics in nickel (II) hexaammino-tetrafluoroborate

Sagnowski

Hodorowicz

Borzęcka-Prokop

1988

Phys. Stat. Sol. (a)

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[Ni(NH3)6](BF4)2 is investigated by a wide‐line NMR technique. The temperature dependences of the second moment of proton and fluorine spectra in the range of 4.2 to 370 K are presented. On the basis of the dynamical model proposed for the crystal lattice of the compound a detailed analysis of the experimental data is made. The axial reorientations of ammonia groups, the tumbling motion of complex hexaammino cations, and the isotropical reorientations of tetrafluoroborate anions are proved to be responsible for the observed effects.

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1H and19F magnetic resonance study on molecular dynamics in nickel (II) hexaammino-tetrafluoroborate

Sagnowski

Hodorowicz

Borzęcka-Prokop

1988

Phys. Stat. Sol. (a)

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Incoherent inelastic and quasielastic neutron scattering with simultaneous neutron diffraction control of phase transitions in [Ni(NH3)6](NO3)2

Belushkin¹,

Janik²,

Janik³

et al. 1983

Physica B+C

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Thermal behaviour of polycrystalline [Ba(H2O)3](ClO4)2 and [Ba(NH3)4](ClO4)2

et al. 2009

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Lattice Dynamics of [Ni(NH₃)₆] (ClO₄)₂, [Ni(NH₃)₆] (BF₄)₂, and [Ni(NH₃)₆] (PF₆)₂

Cited by 3 publications

References 11 publications

1H and19F magnetic resonance study on molecular dynamics in nickel (II) hexaammino-tetrafluoroborate

1H and19F magnetic resonance study on molecular dynamics in nickel (II) hexaammino-tetrafluoroborate

Incoherent inelastic and quasielastic neutron scattering with simultaneous neutron diffraction control of phase transitions in [Ni(NH3)6](NO3)2

Thermal behaviour of polycrystalline [Ba(H2O)3](ClO4)2 and [Ba(NH3)4](ClO4)2

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